University College London
Browse
1/1
6 files

XAFS data at Pd & In K-edges recorded in situ during reduction and ex situ.

dataset
posted on 2023-12-08, 11:29 authored by Andrew BealeAndrew Beale, Lisa Allen, Leila Negahdar

X-ray absorption spectroscopy was performed at Diamond Light Source, UK, at B18 for the Pd/In2O3 & Pd/In2O3/Al2O3 species. Data was collected at the Pd and In K-edges in transmission mode using a QEXAFS setup with fast scanning Si(311) crystal monochromators. The time resolution here was roughly 90 seconds per spectrum. Samples were packed into an in-house custom-made capillary system designed and constructed by Diamond Light Source. 50 mg of 200-300 μm catalyst particles were packed between 3 cm of quartz wool.

Funding

The UK Catalysis Hub -'Core'

Engineering and Physical Sciences Research Council

Find out more...

The UK Catalysis Hub - 'Science': 1 - Optimising, predicting and designing new Catalysts

Engineering and Physical Sciences Research Council

Find out more...

Selective CO2 conversion to renewable methanol through innovative heterogeneous catalyst systems optimized for advanced hydrogenation technologies (microwave, plasma and magnetic induction).

European Commission

Find out more...

History

Usage metrics

    Department of Chemistry

    Licence

    Exports

    RefWorks
    BibTeX
    Ref. manager
    Endnote
    DataCite
    NLM
    DC